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Heating Samples to 2000° C for Scanning Tunneling Microscopy Studies in Ultrahigh Vacuum

Feb 4, 2025

A simple device for heating single-crystal samples to temperatures ≥2000 °C in ultrahigh vacuum that is compatible with the standard sample plates used in a common commercial scanning tunneling microscope (STM) is described.

Heating high melting point samples to higher temperatures than is possible with many existing STM sample holders is necessary to obtain clean, well-ordered surfaces. Results are demonstrated for the (0001) surface of ZrB2, which has a melting point of 3050 °C.

Publication

Authors

Michael Trenary (U. Illinois - Chicago)

Additional Materials

U.S. National Science Foundation and NSF DMREF, Materials for Our Future

This material is based upon work supported by the U.S. National Science Foundation Award No. 2015237. Any opinions, findings, and conclusions or recommendations expressed in this material are those of the author(s) and do not necessarily reflect the views of the U.S. National Science Foundation. This site is maintained collaboratively by principal investigators with NSF DMREF awards, independent of the NSF.